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- W966293793 abstract "The title compound [Cu(Phen)3](CIO4)2(btio)(H2O), where btio = 2-(4'-benzoyloxyl)-4,4,5,5-tetramethylimidazoline-l-oxyl-3-oxide, has been prepared .and structurally characterized by X-ray diffraction. It crystallizes in triclinic, space group P1^- with a = 13.049(4), b= 13.827(5), c = 14.860(5)/A^°, α = 71.736(6), β = 77.076(6), γ= 87.054(6)°, C50H43Cl2CuN8O13, Mr= 1098.36, V= 2481(1)A^°3, Z = 2, Dc = 1.470 g/cm^3,μ(MoKα) = 0.622 mm^-1, F(000) = 1132, the final R = 0.0639 and wR = 0.1473 for 8705 independent reflections with Rint =0.0285. The title compound is composed of [Cu(Phen)3]^2+ moiety, one btio, two perchlorate ions and one water molecule. The copper(Ⅱ) ion is octahedrally coordinated by three 1,10-phenanthroline ligands. The outer sphere consisting of one btio, two perchlorate ions and one water molecule is combined with the inner by hydrogen bonds and electrostatic interactions." @default.
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- W966293793 date "2004-01-01" @default.
- W966293793 modified "2023-09-26" @default.
- W966293793 title "Synthesis and Crystal Structure of a Novel Complex [Cu（Phen）3]（CIO4）2（btio）（H2O）" @default.
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