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- W967382494 abstract "This chapter summarizes the mass and fluid transfer processes that dominate as a solvent passes over particles in a packed column bed during chromatography. The liquid passing through chromatography column is referred to as the mobile phase while, in most cases, the solid particle is called the stationary phase. There are two transport mechanisms in progress during a flow of mobile phase through a packed column bed: the convectional flow around the particles and the diffusion in and out of the pores of the stationary phase. The chapter discusses the composite effects of mass transport of particles in a chromatographic column. For an efficient preparative separation where the objective is to maximize loading and minimize height equivalent to theoretical plates (HETP), it is always worth considering an investigation of pore size dimensions. Along with the pore size of stationary phase and mass transport, other major effects that have to be considered when scaling a preparative separation are heat generated by the friction caused by the eluent passing over stationary phase particles, which in turn reduces the viscosity of the solvent and band broadening at the center of the column." @default.
- W967382494 created "2016-06-24" @default.
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- W967382494 date "2005-01-01" @default.
- W967382494 modified "2023-09-23" @default.
- W967382494 title "Fluid dynamics, mass transport and friction" @default.
- W967382494 doi "https://doi.org/10.1016/b978-185617466-4/50004-9" @default.
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