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- W974842192 abstract "The inter-diffusion of N,N-dimethylformamide solution of Zn(phen)2Cl2 and (NH4)2MS4 (M = W, Mo) in an H-shape tube produced crystals of Zn(phen)2WS4 1 and Zn(phen)2MoS4 2 (phen = 1,10-phenanthroline). The structures of isomorphous complexes 1 and 2 have been determined by X-ray single-crystal structure analyses. Four nitrogen atoms from the phenanthroline ligands and two sulfur atoms from the MS42－ anion forming a distorted octahedron coordinate each zinc atom. Through (-( interactions of adjacent aromatic rings of the phenanthroline ligands, a quasi one-dimensional zigzag-stacking column is formed in each complex. Complex 1 crystallizes in monoclinic space group C2/c, with a = 10.447(8), b = 22.016(9), c = 12.824(8) ?, ( = 103.56(6)°, V = 2867.7(8) ?3, Z = 4, C24H16N4S4WZn, Mr=737.90, Dc = 1.71 g/cm3, F(000) = 1424, ( = 5.25 mm－1, the final R = 0.054 and Rw = 0.075 for 2315 observations with I > 3( (I). Complex 2 crystallizes in monoclinic space group C2/c, with a = 10.410(6), b = 22.095(7), c = 12.830(6) , ( = 103.19(8)°, V = 2873.1(5) 3, Z = 4, C24H16MoN4S4Zn, Mr=649.99, Dc = 1.50 g/cm3, F(000) = 1296, ( = 1.58 mm－1, the final R = 0.072 and Rw = 0.100 for 1631 observations with I > 3((I)." @default.
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- W974842192 date "2001-01-01" @default.
- W974842192 modified "2023-09-28" @default.
- W974842192 title "π—πStacking Force in the Solid Structure of Mixed—Metal complexes：Zn（phen）2MS4（M=W,Mo）" @default.
- W974842192 hasPublicationYear "2001" @default.
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