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- W975920515 abstract "[Objective] This study aimed to establish an electrochemiluminescence method for determining the trace molybdenum content in plant seeds.[Method] The equipment used in this study consists of an electrogenerated reagent system and a flow injection chemiluminescenc detection system.The optimal electric potential,reagent acidity,sample solution flow rate,as well as the concentration and alkalinity of the luminal were screened to measure the trace molybdenum content in plant seeds.[Result] The unstable molybdenum(III) was on-line electrogenerated from molybdenum(VI) via controlled potential electrolysis technique using a homemade flow-through carbon electrolytic cell at the potential of-0.60 V(vs Ag/AgCl).The method allows the determination of 5.0×10-10-5.0×10-7 g/ml molybdenum with a detection limit of 5×10-11 g/ml molybdenum.The relative standard deviation is 2.6% for the 1.0×10-9 g/ml molybdenum solution in 11 measurements.[Conclusion] Compared with previous methods,this electrochemiluminescence method not only improved the selectivity,but also avoided the use of toxic reagent mercury." @default.
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- W975920515 date "2012-01-01" @default.
- W975920515 modified "2023-09-23" @default.
- W975920515 title "Determination of trace molybdenum in plant seeds by electrochemiluminescence method." @default.
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